有现成的文献报道的成熟路线,需要用到臭氧。
Name:dispiro[adamantane-2,3′-[1,2,4]trioxolane-5′,1”-cyclohexan]-4”-ol
Chemical Formula: C16H24O4
Molecular Weight: 280.3640
m/z: 280.1675 (100.0%), 281.1708 (17.3%), 282.1742 (1.4%)
Elemental Analysis: C, 68.55; H, 8.63; O, 22.83