天然白藜芦醇做一步氢化反应,可提供原料
Procedure:
To a solution of resveratrol (114 g, 500 mM) in 500 ml EtOAc and 200 ml EtOH, Pd/C was added portion-wisely at r.t.. The mixture was stirred for 24 hours at r.t. under hydrogen.
The mixture was filtered with silica gel to remove Pd/C. The filtrate was concentrated to give a solid. The solid was washed by EtOAc (50 ml) and the mixture was suction filtered to give a white solid. The solid was dried by vaccum for 3h. The solid was powdered and sifted through 100-mesh sieve.
中文名称:二氢藜芦醇中文
同义词:二氢白藜芦醇;二氢藜芦醇
英文名称:Dihydroresveratrol
英文同义词:Dihydroresveratrol;3,4′,5-Trihydroxybibenzyl;4-[2-(3,5-Dihydroxyphenyl)ethyl]phenol;5-[2-(4-Hydroxyphenyl)ethyl]benChemicalbookzene-1,3-diol;Dihydroresveratol;α,β-Dihydrostilbene-3,4′,5-triol;5-[2-(4-hydroxyphenyl)ethyl]-1,3-benzenediol;3,5,4′-Trihydroxybibenzyl
CAS号:58436-28-5
分子式:C14H14O3
分子量:230.262